Description of Individual Course Units
Course Unit CodeCourse Unit TitleType of Course UnitYear of StudySemesterNumber of ECTS Credits
300001312005GENERAL CHEMISTRY-ICompulsory115
Level of Course Unit
First Cycle and Second Cycle
Objectives of the Course
Analytical Chemistry-II examines the analyses based upon the seperation and recognition of a sample belonging to a matter. Within this context, it is aimed to educate people, that have basic knowledge and laboratory practice based upon acid-base, precipitation, complexation and redox reaction, is capable of developing a research project devoted to the calitative analysis of pharmaceutical preparations and medical products by producing an idea for corresponding subjects in future and able to produce solutions for the problems of pharmaceutical industries.
Name of Lecturer(s)
Prof. Dr. K. Arzum ERDEM GÜRSAN, Prof. Dr. Özlem SÖĞÜT, Prof. Dr. Dr. M. Emrah KILINÇ, Assoc. Prof. Dr. Dilşat ARIKSOYSAL, Assoc Prof. Dr. Pınar KARA KADAYIFCILAR,Assoc. Prof. Dr. Hakan KARADENİZ
Learning Outcomes
1To be able to comprehend the descriptions and methods based upon quantitative analysis.
2To be able to identify the sources of errors at quantitative analysis and to command on the reducing of errors.
3To be able to comprehend the basic concepts at gravimetric analysis, to make gravimetric calculations.
4To gain the skill of commending on acid-base (neutralization) titrations and making calculations
5To gain the skill of commanding and making calculation for precipitation titration.
6To gain the skill of commanding and making calculation for complexation titration.
7To gain the skill of commanding and making calculation for redox reaction.
Mode of Delivery
Face to Face
Prerequisites and co-requisities
None
Recommended Optional Programme Components
To be successful at General Chemistry-I General Chemistry-II and Analytical Chemistry I lessons
Course Contents
Volumetric analysis(titrations) about acids, bases, salts, buffers, polyacids, polibases and their calculations, precipitation titrations and related calculations, complexation titrations, redox titrations and applications related to these subjects, to comprehension of the importance in daily life.
Weekly Detailed Course Contents
WeekTheoreticalPracticeLaboratory
1Introduction, Basics of cantitative analysis methods I. Methods of explanation the analysis errors Demonstration of Analytical Chemistry II laboratory
2Introduction, II. Basics of Gravimetry and volumetry Introduction Exercises Laboratory safety
3Gravimetry, I. Descriptions II. Finding the gravimetric factor and calculations based upon the gravimetric analysis The constitution of aparaturs used in Analytical Chemistry II laboratory and make the titrations of samples.
4Neutralization titrations, I.Introduction, Descriptions II. Colorful indicators Acidimetry-Alkalimetry a) Preparation of 0.5L 0.1NHCl solutions b) Adjustment
5Neutralization Titrations, a.Transition intervals of indicators b. Selection of indicators Acidimetry-Alkalimetry a) NaOH quantity determination, b) 0.5L 0.1N NaOH solution preparation and adjustment with calibrated 0.1N HCl
6Neutralization titrations, Neutralization titrations-IAcidimetry-Alkalimetry a)Acetic acid quantity determination, b)HCl+H3PO4 mixture quantity determination
7Neutralization titrations, Neutralization titrations-II Exercises and solutions Precipitation Titrations (Arjantometry) a) Chloride quantity determination (Mohr method) b) Bromide quantity determination (Volhard method)
8Precipitation titrations I. Introduction and descriptions II. Mohr methodComplexometry a) 0.5L, 0.01N EDTA Solution preparations b) b)Identification of degrees of hardness of water c) c) Mg2+ quantity identification
9Precipitation titrations III. Volhard method IV. Other methods exercises and their solutions MIDTERM WEEK Redox titrations (Manganymetry) a) 0.5L, 0.1N KmnO4 solution preparation b) Adjustment
10Complexation Titrations I.Introduction and descriptions II.Formation of colorful complexes III.Complexation titrationsRedox titrations (manganymetry) a) Fe2+ quantity identification b) NaNO2 quantity identification
11Complexation titrations IV.Selection of indicator 1.Metal indicators 2.Fotometric titrations 3.Potentiometric titrations Exercises and solutions Redox titrations (Iodometry) a) 0.5L 0.05N Na2S2O3 solution preparation b) Adjustment
12Redox titrations I.Introduction and descriptions II.Mechanishm of redox titrations Redox titrations (iodometry) a) Fe3+ quantity identification b) Cu2+ quantity identification
13Redox titrations II.Identification of equivalence point a.Potantiometric methods b.Internal redox indicators Potentiometry
14Redox Titrations c. Varied methods for identification of final point III. Pre-oxidation and pre-reduction Final Examination
15Redox titrations IV.Some important practical advices Exercisesand their answers
16Final Examination
Recommended or Required Reading
1.Prof. Dr. Aycıl Kayalı, Analytical Chemistry I for pharmacists, E.Ü. Pharmacy Faculty, Basic Pharmacy Sciences Department, Department of Analytical Chemistry. 2.Douglas A. Skoog, Donald M. West, F. James Holler, Basics of Analytical Chemistry I and II, Translation editors Prof. Dr. Esma Kılıç, Prof. Dr. Fitnat Köseoğlu, Bilişim Yayıncılık, 7. Baskı, Ankara, 1999. 3.Prof. Dr. Aycıl Kayalı, Prof. Dr. M.E.Şengün Özsöz, Assoc. Prof. Cengiz Yalçınkaya, Assoc. Prof. Cengiz Kurdoğlu, Assoc. Prof. Özlem Söğüt Ertaş, Assoc. Prof. M. Emrah Kılınç, Analytical Chemistry I Laboratory, Book of Quantitative analysis, E.Ü. Pharmacy Faculty, Basic Pharmacy Sciences Department, Department of Analytical Chemistry. 4.Daniel C Haris, Book of Analytical Chemistry, Translation Editors Prof. Dr. Güler Somer, Prof. Dr. Ali Osman Solak, Prof.Dr. Ali Reber Türker, Prof. Dr. Esma Kılıç,Prof. Dr. Fitnat Köseoğlu, Prof. Dr.Latif Elçi, Prof. Dr.Mehmet Doğan, Prof. Dr.Mustafa Özcimder, Prof. Dr.Mustafa Özdemir, Prof. Dr.Serdar Ateş, Prof. Dr.Şeref Kunç, Prof. Dr.Şeref Güçer, Gazi Bureau Bookshop, Ankara, 1994. Kitabevi, Ankara, 1994.
Planned Learning Activities and Teaching Methods
Activities are given in detail in the section of "Assessment Methods and Criteria" and "Workload Calculation"
Assessment Methods and Criteria
Term (or Year) Learning ActivitiesQuantityWeight
SUM0
End Of Term (or Year) Learning ActivitiesQuantityWeight
SUM0
SUM0
Language of Instruction
Turkish
Work Placement(s)
None
Workload Calculation
ActivitiesNumberTime (hours)Total Work Load (hours)
Midterm Examination122
Final Examination122
Attending Lectures14228
Practice14342
Self Study12020
Individual Study for Mid term Examination12020
Individual Study for Final Examination14747
Laboratory Midterm Examination111
Post Quiz400
TOTAL WORKLOAD (hours)162
Contribution of Learning Outcomes to Programme Outcomes
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* Contribution Level : 1 Very low 2 Low 3 Medium 4 High 5 Very High
 
Ege University, Bornova - İzmir / TURKEY • Phone: +90 232 311 10 10 • e-mail: intrec@mail.ege.edu.tr