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Description of Individual Course Units| Course Unit Code | Course Unit Title | Type of Course Unit | Year of Study | Semester | Number of ECTS Credits | | 300002402006 | ANALYTICAL CHEMISTRY II | Compulsory | 2 | 4 | 5 |
| | Level of Course Unit | | First Cycle and Second Cycle | | Language of Instruction | | Turkish | | Objectives of the Course | | Analytical Chemistry-II examines the instrumental analysis of chemical analysis, the precise quantification of species in a sample and the method validation. In this context, atomic subject previously given in General Chemistry I course, General Chemistry II and Analytical Chemistry I courses given in the acid-base, precipitation, complexation and redox topics, as well as laboratory practice, to produce ideas about pharmaceuticals and medicinal products to develop research projects for quantitative analysis of instruments and to produce solutions to the problems of the pharmaceutical industry. | | Name of Lecturer(s) | | Prof. Dr. M. Emrah KILINÇ, Prof. Dr. Özlem SÖĞÜT, Prof. Dr. K. Arzum ERDEM GÜRSAN, Prof. Dr. Pınar KARA KADAYIFCILAR, Doç Dr. Dilşat ARIKSOYSAL, , Doç. Dr. Hakan KARADENİZ | | Learning Outcomes | | 1 | To be able to comprehend the definitions and methods of instrumental quantitative analysis and also the basics of measurement. | | 2 | To be able to classify instrumental analysis methods. | | 3 | To gain the ability to comment on the application areas of instrumental analysis methods | | 4 | To be able to explain the basic principles of spectrometric methods and to give examples of application areas. | | 5 | To be able to explain the use of separation methods, to give examples of application areas. | | 6 | To be able to explain the use of electrometric methods, to give examples of application areas. | | 7 | To be able to explain the use of other instrumental methods, to give examples of application areas. |
| | Mode of Delivery | | Face to Face | | Prerequisites and co-requisities | | None | | Recommended Optional Programme Components | | To be successful at General Chemistry-I General Chemistry-II and Analytical Chemistry I lessons | | Course Contents | | Validation of analytical methods, instrumental analysis methods, spectrometric methods, separation methods, electrometric methods and other instrumental methods, and applications and calculations related to these issues, understanding of their importance in daily life and pharmacy. | | Weekly Detailed Course Contents | |
| 1 | Definition of analysis and method selection
| Demonstration of Analytical Chemistry II laboratory | | | 2 | Method validation | Laboratory safety | | | 3 | Sources of errors in chemical analysis, applications in quantitative analysis | The constitution of aparaturs used in Analytical Chemistry II laboratory and make the titrations of samples. | | | 4 | Introduction to spectroscopic methods and general information
| Acidimetry-Alkalimetry
a) Preparation of 0.5L 0.1NHCl solutions
b) Adjustment | | | 5 | Atomic and molecular absorption, UV and GB absorption, Absorption measuring devices, Lambert-Beer Law | Acidimetry-Alkalimetry
a) NaOH quantity determination,
b) 0.5L 0.1N NaOH solution preparation and
adjustment with calibrated 0.1N HCl
| | | 6 | Qualitative analysis with spectrophotometer, IR spectroscopy, Fourier Transform IR spectrophotometer, photoluminescence, chemiluminescence, turbidimetry, nephelometry, fluorescence, phosphorescence, refractometry, polarimertry general information. | Acidimetry-Alkalimetry
a)Acetic acid quantity determination,
b)HCl+H3PO4 mixture quantity determination
| | | 7 | Atomic absorption (AAS), atomic emission (AES) and atomic fluorescence (AFS) spectroscopy, qualitative and quantitative analysis
| Precipitation Titrations (Arjantometry)
a) Chloride quantity determination (Mohr method)
b) Bromide quantity determination (Volhard method) | | | 8 | General information about separation methods | Complexometry
a) 0.5L, 0.01N EDTA Solution preparations
b) b)Identification of degrees of hardness of water
c) c) Mg2+ quantity identification
| | | 9 | Liquid chromatography
MIDTERM WEEK
| Redox titrations (Manganymetry)
a) 0.5L, 0.1N KmnO4 solution preparation
b) Adjustment | | | 10 | Gas chromatography | Redox titrations (manganymetry)
a) Fe2+ quantity identification
b) NaNO2 quantity identification
| | | 11 | Introduction to electroanalytical methods | Redox titrations (Iodometry)
a) 0.5L 0.05N Na2S2O3 solution preparation
b) Adjustment | | | 12 | Information about voltammetry, amperometry, potentiometric methods, types and other electroanalytical methods
| Redox titrations (iodometry)
a) Fe3+ quantity identification
b) Cu2+ quantity identification
| | | 13 | Examples of applications of electroanalytical methods in the field of pharmacy
| Potentiometry | | | 14 | Other methods used in instrumental analysis
| Final Examination | | | 15 | Excercises. Final Examination | | |
| | Recommended or Required Reading | | 1.Prof. Dr. Aycıl Kayalı, Analytical Chemistry I for pharmacists, E.Ü. Pharmacy Faculty, Basic Pharmacy Sciences Department, Department of Analytical Chemistry.
2.Douglas A. Skoog, Donald M. West, F. James Holler, Basics of Analytical Chemistry I and II, Translation editors Prof. Dr. Esma Kılıç, Prof. Dr. Fitnat Köseoğlu, Bilişim Yayıncılık, 7. Baskı, Ankara, 1999.
3.Prof. Dr. Aycıl Kayalı, Prof. Dr. M.E.Şengün Özsöz, Assoc. Prof. Cengiz Yalçınkaya, Assoc. Prof. Cengiz Kurdoğlu, Assoc. Prof. Özlem Söğüt Ertaş, Assoc. Prof. M. Emrah Kılınç, Analytical Chemistry I Laboratory, Book of Quantitative analysis, E.Ü. Pharmacy Faculty, Basic Pharmacy Sciences Department, Department of Analytical Chemistry.
4.Daniel C Harris, Book of Analytical Chemistry, Translation Editors Prof. Dr. Güler Somer, Prof. Dr. Ali Osman Solak, Prof.Dr. Ali Rehber Türker, Prof. Dr. Esma Kılıç,Prof. Dr. Fitnat Köseoğlu, Prof. Dr.Latif Elçi, Prof. Dr.Mehmet Doğan, Prof. Dr.Mustafa Özcimder, Prof. Dr.Mustafa Özdemir, Prof. Dr.Serdar Ateş, Prof. Dr.Şeref Kunç, Prof. Dr.Şeref Güçer, Gazi Bureau Bookshop, Ankara, 1994.
| | Planned Learning Activities and Teaching Methods | | | Assessment Methods and Criteria | |
| Midterm Examination | 1 | 100 | | SUM | 100 | |
| Final Sınavı | 1 | 100 | | SUM | 100 | | Term (or Year) Learning Activities | 40 | | End Of Term (or Year) Learning Activities | 60 | | SUM | 100 |
| | Work Placement(s) | | None |
| | Workload Calculation | |
| Midterm Examination | 1 | 2 | 2 | | Final Examination | 1 | 2 | 2 | | Attending Lectures | 14 | 2 | 28 | | Practice | 14 | 3 | 42 | | Self Study | 1 | 20 | 20 | | Individual Study for Mid term Examination | 1 | 20 | 20 | | Individual Study for Final Examination | 1 | 47 | 47 | | Laboratory Midterm Examination | 1 | 1 | 1 | | Post Quiz | 4 | 0 | 0 | |
| Contribution of Learning Outcomes to Programme Outcomes | | LO1 | | | | | | | 5 | 5 | 4 | 4 | 5 | | | | | | | | | | 5 | | LO2 | | | | | | | 5 | 5 | 5 | 5 | 5 | | | | | | | | | | 5 | | LO3 | | | | | | | 5 | 5 | 5 | 5 | 5 | | | | | | | | | | 5 | | LO4 | | | | | | | 5 | 5 | 5 | 5 | 5 | | | | | | | | | | 5 | | LO5 | | | | | | | 5 | 5 | 5 | 5 | 5 | | | | | | | | | | 5 | | LO6 | | | | | | | 5 | 5 | 5 | 5 | 5 | | | | | | | | | | 5 | | LO7 | | | | | | | 5 | 5 | 5 | 5 | 5 | | | | | | | | | | 5 |
| | * Contribution Level : 1 Very low 2 Low 3 Medium 4 High 5 Very High |
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| Ege University, Bornova - İzmir / TURKEY • Phone: +90 232 311 10 10 • e-mail: intrec@mail.ege.edu.tr |
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