EGE UNIVERSITY Lifelong Learning Programme

Description of Individual Course Units

Course Unit Code	Course Unit Title	Type of Course Unit	Year of Study	Semester	Number of ECTS Credits
300002402006	ANALYTICAL CHEMISTRY II	Compulsory	2	4	5

Level of Course Unit

First Cycle and Second Cycle

Objectives of the Course

Analytical Chemistry-II examines the analyses based upon the seperation and recognition of a sample belonging to a matter. Within this context, it is aimed to educate people, that have basic knowledge and laboratory practice based upon acid-base, precipitation, complexation and redox reaction, is capable of developing a research project devoted to the calitative analysis of pharmaceutical preparations and medical products by producing an idea for corresponding subjects in future and able to produce solutions for the problems of pharmaceutical industries.

Name of Lecturer(s)

Prof. Dr. K. Arzum ERDEM GÜRSAN, Prof. Dr. Özlem SÖĞÜT, Prof. Dr. Dr. M. Emrah KILINÇ, Assoc. Prof. Dr. Dilşat ARIKSOYSAL, Assoc Prof. Dr. Pınar KARA KADAYIFCILAR,Assoc. Prof. Dr. Hakan KARADENİZ

Learning Outcomes

1	To be able to comprehend the descriptions and methods based upon quantitative analysis.
2	To be able to identify the sources of errors at quantitative analysis and to command on the reducing of errors.
3	To be able to comprehend the basic concepts at gravimetric analysis, to make gravimetric calculations.
4	To gain the skill of commending on acid-base (neutralization) titrations and making calculations
5	To gain the skill of commanding and making calculation for precipitation titration.
6	To gain the skill of commanding and making calculation for complexation titration.
7	To gain the skill of commanding and making calculation for redox reaction.

Mode of Delivery

Face to Face

Prerequisites and co-requisities

None

Recommended Optional Programme Components

To be successful at General Chemistry-I General Chemistry-II and Analytical Chemistry I lessons

Course Contents

Volumetric analysis(titrations) about acids, bases, salts, buffers, polyacids, polibases and their calculations, precipitation titrations and related calculations, complexation titrations, redox titrations and applications related to these subjects, to comprehension of the importance in daily life.

Weekly Detailed Course Contents

Week	Theoretical	Practice	Laboratory
1	Introduction, Basics of cantitative analysis methods I. Methods of explanation the analysis errors	Demonstration of Analytical Chemistry II laboratory
2	Introduction, II. Basics of Gravimetry and volumetry Introduction Exercises	Laboratory safety
3	Gravimetry, I. Descriptions II. Finding the gravimetric factor and calculations based upon the gravimetric analysis	The constitution of aparaturs used in Analytical Chemistry II laboratory and make the titrations of samples.
4	Neutralization titrations, I.Introduction, Descriptions II. Colorful indicators	Acidimetry-Alkalimetry a) Preparation of 0.5L 0.1NHCl solutions b) Adjustment
5	Neutralization Titrations, a.Transition intervals of indicators b. Selection of indicators	Acidimetry-Alkalimetry a) NaOH quantity determination, b) 0.5L 0.1N NaOH solution preparation and adjustment with calibrated 0.1N HCl
6	Neutralization titrations, Neutralization titrations-I	Acidimetry-Alkalimetry a)Acetic acid quantity determination, b)HCl+H3PO4 mixture quantity determination
7	Neutralization titrations, Neutralization titrations-II Exercises and solutions	Precipitation Titrations (Arjantometry) a) Chloride quantity determination (Mohr method) b) Bromide quantity determination (Volhard method)
8	Precipitation titrations I. Introduction and descriptions II. Mohr method	Complexometry a) 0.5L, 0.01N EDTA Solution preparations b) b)Identification of degrees of hardness of water c) c) Mg2+ quantity identification
9	Precipitation titrations III. Volhard method IV. Other methods exercises and their solutions MIDTERM WEEK	Redox titrations (Manganymetry) a) 0.5L, 0.1N KmnO4 solution preparation b) Adjustment
10	Complexation Titrations I.Introduction and descriptions II.Formation of colorful complexes III.Complexation titrations	Redox titrations (manganymetry) a) Fe2+ quantity identification b) NaNO2 quantity identification
11	Complexation titrations IV.Selection of indicator 1.Metal indicators 2.Fotometric titrations 3.Potentiometric titrations Exercises and solutions	Redox titrations (Iodometry) a) 0.5L 0.05N Na2S2O3 solution preparation b) Adjustment
12	Redox titrations I.Introduction and descriptions II.Mechanishm of redox titrations	Redox titrations (iodometry) a) Fe3+ quantity identification b) Cu2+ quantity identification
13	Redox titrations II.Identification of equivalence point a.Potantiometric methods b.Internal redox indicators	Potentiometry
14	Redox Titrations c. Varied methods for identification of final point III. Pre-oxidation and pre-reduction	Final Examination
15	Redox titrations IV.Some important practical advices Exercisesand their answers
16	Final Examination

Recommended or Required Reading

1.Prof. Dr. Aycıl Kayalı, Analytical Chemistry I for pharmacists, E.Ü. Pharmacy Faculty, Basic Pharmacy Sciences Department, Department of Analytical Chemistry. 2.Douglas A. Skoog, Donald M. West, F. James Holler, Basics of Analytical Chemistry I and II, Translation editors Prof. Dr. Esma Kılıç, Prof. Dr. Fitnat Köseoğlu, Bilişim Yayıncılık, 7. Baskı, Ankara, 1999. 3.Prof. Dr. Aycıl Kayalı, Prof. Dr. M.E.Şengün Özsöz, Assoc. Prof. Cengiz Yalçınkaya, Assoc. Prof. Cengiz Kurdoğlu, Assoc. Prof. Özlem Söğüt Ertaş, Assoc. Prof. M. Emrah Kılınç, Analytical Chemistry I Laboratory, Book of Quantitative analysis, E.Ü. Pharmacy Faculty, Basic Pharmacy Sciences Department, Department of Analytical Chemistry. 4.Daniel C Haris, Book of Analytical Chemistry, Translation Editors Prof. Dr. Güler Somer, Prof. Dr. Ali Osman Solak, Prof.Dr. Ali Reber Türker, Prof. Dr. Esma Kılıç,Prof. Dr. Fitnat Köseoğlu, Prof. Dr.Latif Elçi, Prof. Dr.Mehmet Doğan, Prof. Dr.Mustafa Özcimder, Prof. Dr.Mustafa Özdemir, Prof. Dr.Serdar Ateş, Prof. Dr.Şeref Kunç, Prof. Dr.Şeref Güçer, Gazi Bureau Bookshop, Ankara, 1994. Kitabevi, Ankara, 1994.

Planned Learning Activities and Teaching Methods

Activities are given in detail in the section of "Assessment Methods and Criteria" and "Workload Calculation"

Assessment Methods and Criteria

Term (or Year) Learning Activities	Quantity	Weight
SUM		0
End Of Term (or Year) Learning Activities	Quantity	Weight
SUM		0
SUM		0

Language of Instruction

Turkish

Work Placement(s)

None

Workload Calculation

Activities	Number	Time (hours)	Total Work Load (hours)
Midterm Examination	1	2	2
Final Examination	1	2	2
Attending Lectures	14	2	28
Practice	14	3	42
Self Study	1	20	20
Individual Study for Mid term Examination	1	20	20
Individual Study for Final Examination	1	47	47
Laboratory Midterm Examination	1	1	1
Post Quiz	4	0	0
TOTAL WORKLOAD (hours)			162

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