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Description of Individual Course UnitsCourse Unit Code | Course Unit Title | Type of Course Unit | Year of Study | Semester | Number of ECTS Credits | 300002402006 | ANALYTICAL CHEMISTRY II | Compulsory | 2 | 4 | 5 |
| Level of Course Unit | First Cycle and Second Cycle | Objectives of the Course | Analytical Chemistry-II examines the analyses based upon the seperation and recognition of a sample belonging to a matter. Within this context, it is aimed to educate people, that have basic knowledge and laboratory practice based upon acid-base, precipitation, complexation and redox reaction, is capable of developing a research project devoted to the calitative analysis of pharmaceutical preparations and medical products by producing an idea for corresponding subjects in future and able to produce solutions for the problems of pharmaceutical industries. | Name of Lecturer(s) | Prof. Dr. K. Arzum ERDEM GÜRSAN, Prof. Dr. Özlem SÖĞÜT, Prof. Dr. Dr. M. Emrah KILINÇ, Assoc. Prof. Dr. Dilşat ARIKSOYSAL, Assoc Prof. Dr. Pınar KARA KADAYIFCILAR,Assoc. Prof. Dr. Hakan KARADENİZ | Learning Outcomes | 1 | To be able to comprehend the descriptions and methods based upon quantitative analysis. | 2 | To be able to identify the sources of errors at quantitative analysis and to command on the reducing of errors. | 3 | To be able to comprehend the basic concepts at gravimetric analysis, to make gravimetric calculations. | 4 | To gain the skill of commending on acid-base (neutralization) titrations and making calculations | 5 | To gain the skill of commanding and making calculation for precipitation titration. | 6 | To gain the skill of commanding and making calculation for complexation titration. | 7 | To gain the skill of commanding and making calculation for redox reaction. |
| Mode of Delivery | Face to Face | Prerequisites and co-requisities | None | Recommended Optional Programme Components | To be successful at General Chemistry-I General Chemistry-II and Analytical Chemistry I lessons | Course Contents | Volumetric analysis(titrations) about acids, bases, salts, buffers, polyacids, polibases and their calculations, precipitation titrations and related calculations, complexation titrations, redox titrations and applications related to these subjects, to comprehension of the importance in daily life. | Weekly Detailed Course Contents | |
1 | Introduction,
Basics of cantitative analysis methods
I. Methods of explanation the analysis errors
| Demonstration of Analytical Chemistry II laboratory | | 2 | Introduction,
II. Basics of Gravimetry and volumetry
Introduction Exercises
| Laboratory safety | | 3 | Gravimetry,
I. Descriptions
II. Finding the gravimetric factor and calculations based upon the gravimetric analysis
| The constitution of aparaturs used in Analytical Chemistry II laboratory and make the titrations of samples. | | 4 | Neutralization titrations,
I.Introduction, Descriptions
II. Colorful indicators
| Acidimetry-Alkalimetry
a) Preparation of 0.5L 0.1NHCl solutions
b) Adjustment | | 5 | Neutralization Titrations,
a.Transition intervals of indicators
b. Selection of indicators
| Acidimetry-Alkalimetry
a) NaOH quantity determination,
b) 0.5L 0.1N NaOH solution preparation and
adjustment with calibrated 0.1N HCl
| | 6 | Neutralization titrations,
Neutralization titrations-I | Acidimetry-Alkalimetry
a)Acetic acid quantity determination,
b)HCl+H3PO4 mixture quantity determination
| | 7 | Neutralization titrations,
Neutralization titrations-II
Exercises and solutions
| Precipitation Titrations (Arjantometry)
a) Chloride quantity determination (Mohr method)
b) Bromide quantity determination (Volhard method) | | 8 | Precipitation titrations
I. Introduction and descriptions
II. Mohr method | Complexometry
a) 0.5L, 0.01N EDTA Solution preparations
b) b)Identification of degrees of hardness of water
c) c) Mg2+ quantity identification
| | 9 | Precipitation titrations
III. Volhard method
IV. Other methods exercises and their solutions
MIDTERM WEEK
| Redox titrations (Manganymetry)
a) 0.5L, 0.1N KmnO4 solution preparation
b) Adjustment | | 10 | Complexation Titrations
I.Introduction and descriptions
II.Formation of colorful complexes
III.Complexation titrations | Redox titrations (manganymetry)
a) Fe2+ quantity identification
b) NaNO2 quantity identification
| | 11 | Complexation titrations
IV.Selection of indicator
1.Metal indicators
2.Fotometric titrations
3.Potentiometric titrations
Exercises and solutions
| Redox titrations (Iodometry)
a) 0.5L 0.05N Na2S2O3 solution preparation
b) Adjustment | | 12 | Redox titrations
I.Introduction and descriptions
II.Mechanishm of redox titrations
| Redox titrations (iodometry)
a) Fe3+ quantity identification
b) Cu2+ quantity identification
| | 13 | Redox titrations
II.Identification of equivalence point
a.Potantiometric methods
b.Internal redox indicators
| Potentiometry | | 14 | Redox Titrations
c. Varied methods for identification of final point
III. Pre-oxidation and pre-reduction
| Final Examination | | 15 | Redox titrations
IV.Some important practical advices
Exercisesand their answers
| | | 16 | Final Examination | | |
| Recommended or Required Reading | 1.Prof. Dr. Aycıl Kayalı, Analytical Chemistry I for pharmacists, E.Ü. Pharmacy Faculty, Basic Pharmacy Sciences Department, Department of Analytical Chemistry.
2.Douglas A. Skoog, Donald M. West, F. James Holler, Basics of Analytical Chemistry I and II, Translation editors Prof. Dr. Esma Kılıç, Prof. Dr. Fitnat Köseoğlu, Bilişim Yayıncılık, 7. Baskı, Ankara, 1999.
3.Prof. Dr. Aycıl Kayalı, Prof. Dr. M.E.Şengün Özsöz, Assoc. Prof. Cengiz Yalçınkaya, Assoc. Prof. Cengiz Kurdoğlu, Assoc. Prof. Özlem Söğüt Ertaş, Assoc. Prof. M. Emrah Kılınç, Analytical Chemistry I Laboratory, Book of Quantitative analysis, E.Ü. Pharmacy Faculty, Basic Pharmacy Sciences Department, Department of Analytical Chemistry.
4.Daniel C Haris, Book of Analytical Chemistry, Translation Editors Prof. Dr. Güler Somer, Prof. Dr. Ali Osman Solak, Prof.Dr. Ali Reber Türker, Prof. Dr. Esma Kılıç,Prof. Dr. Fitnat Köseoğlu, Prof. Dr.Latif Elçi, Prof. Dr.Mehmet Doğan, Prof. Dr.Mustafa Özcimder, Prof. Dr.Mustafa Özdemir, Prof. Dr.Serdar Ateş, Prof. Dr.Şeref Kunç, Prof. Dr.Şeref Güçer, Gazi Bureau Bookshop, Ankara, 1994.
Kitabevi, Ankara, 1994.
| Planned Learning Activities and Teaching Methods | Activities are given in detail in the section of "Assessment Methods and Criteria" and "Workload Calculation" | Assessment Methods and Criteria | | Language of Instruction | Turkish | Work Placement(s) | None |
| Workload Calculation | |
Midterm Examination | 1 | 2 | 2 | Final Examination | 1 | 2 | 2 | Attending Lectures | 14 | 2 | 28 | Practice | 14 | 3 | 42 | Self Study | 1 | 20 | 20 | Individual Study for Mid term Examination | 1 | 20 | 20 | Individual Study for Final Examination | 1 | 47 | 47 | Laboratory Midterm Examination | 1 | 1 | 1 | Post Quiz | 4 | 0 | 0 | |
Contribution of Learning Outcomes to Programme Outcomes | LO1 | | | | | | | | | | | | | | | | | | | | | | LO2 | | | | | | | | | | | | | | | | | | | | | | LO3 | | | | | | | | | | | | | | | | | | | | | | LO4 | | | | | | | | | | | | | | | | | | | | | | LO5 | | | | | | | | | | | | | | | | | | | | | | LO6 | | | | | | | | | | | | | | | | | | | | | | LO7 | | | | | | | | | | | | | | | | | | | | | |
| * Contribution Level : 1 Very low 2 Low 3 Medium 4 High 5 Very High |
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Ege University, Bornova - İzmir / TURKEY • Phone: +90 232 311 10 10 • e-mail: intrec@mail.ege.edu.tr |
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