Description of Individual Course Units
Course Unit CodeCourse Unit TitleType of Course UnitYear of StudySemesterNumber of ECTS Credits
404003692006INTRODUCTION TO SEPARATION METHODSElective356
Level of Course Unit
First Cycle
Objectives of the Course
The aim of this course is to teach the basic concepts and principles of separation techniques which are used the elimination of some interferences in real samples.
Name of Lecturer(s)
Prof. Dr. F. Nil ERTAŞ, Assoc. Prof. Dr.Müşerref ARDA
Learning Outcomes
1Being able to understand the importance of separation techniques.
2Being able to comprehend the basic concepts and features of separation techniques
3Being able to select suitable separation techniques for interference problem.
4Being able to solve the problem using classic separation techniques.
5Being able to know the chromatographic separation techniques and comprehend the applications area .
6Being able to compare of the used techniques according to advantages and disadvantages
7Being able to make a group or individual studies,
8Being able to apply modern techniques and to follow the new applications.
Mode of Delivery
Face to Face
Prerequisites and co-requisities
None
Recommended Optional Programme Components
None
Course Contents
The importance and categorize of separation techniques,Distilation, precipatition, liquid-liquid extraction and techniques, ion exchange and separation by resins, chromatographic techniques and classificitation, paper chromatography, thin layer chromatography, gas chromatography and high pressure liquid chromatography.
Weekly Detailed Course Contents
WeekTheoreticalPracticeLaboratory
1Introduction to separation techniques, interference effects, masking and to separate with precipitation
2The principles of distillation and distillation techniques
3Separation with liquid-liquid extraction, extraction yield, exactness of extraction
4liquid-liquid extraction techniques
5Solid phase extraction (SPE)
6Separation with ion exchanger
7Application of ion exchangers
8Mid-term exam
9Introduction to the chromatographic techniques: The principles of chromatographic techniques, definition and classification of the chromatography
10Bant broading and column efficency, application of the chromatography
11Paper chromatography and applications
12Thin layer chromatography and applications
13Gas chromatogaphy: instrumentation of gas-liquid chromatography chromatographic columns, stationary phases, dedectors and applications
14High performance liquid chromatography, high performance adsorpton chromatography, high performance on Exchange chromatography
15High performance size exlusion chromatography and comparison of the HPLC and GC
16Final exam
Recommended or Required Reading
Course Book(s): 1-Skoog, D. A., Holler, F. J., Nieman, T. A. (1998). Enstrumental Analiz İlkeleri. Fifth edition. Saunders College Publishing 2- Skoog, D. A., West, M. D., Nieman, T. A. (1996). Fundamentals of Analytical Chemistry. Seventh edition. Saunders College Publishing 3-Chemical Analysis, A series of monographs on analytical chemistry and its applications, J.D.Winefordner (Editor),(2003), Vol162, Wiley Interscience Publishing
Planned Learning Activities and Teaching Methods
Activities are given in detail in the section of "Assessment Methods and Criteria" and "Workload Calculation"
Assessment Methods and Criteria
Term (or Year) Learning ActivitiesQuantityWeight
SUM0
End Of Term (or Year) Learning ActivitiesQuantityWeight
SUM0
SUM0
Language of Instruction
Turkish
Work Placement(s)
None
Workload Calculation
ActivitiesNumberTime (hours)Total Work Load (hours)
Midterm Examination122
Final Examination122
Attending Lectures14342
Experiment14228
Report Preparation14228
Self Study14228
Individual Study for Mid term Examination12020
Individual Study for Final Examination14040
TOTAL WORKLOAD (hours)190
Contribution of Learning Outcomes to Programme Outcomes
PO
1
PO
2
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3
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4
PO
5
PO
6
PO
7
PO
8
PO
9
PO
10
PO
11
PO
12
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13
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14
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15
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16
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17
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18
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19
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20
PO
21
PO
22
LO14   5                 
LO2 5   5  4             
LO3           5   4      
LO4    4        4        
LO5      5       3       
LO6         4            
LO7       5              
LO8                      
* Contribution Level : 1 Very low 2 Low 3 Medium 4 High 5 Very High
 
Ege University, Bornova - İzmir / TURKEY • Phone: +90 232 311 10 10 • e-mail: intrec@mail.ege.edu.tr